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An experimental study of heat transfer was carried out in the hyper-vapotron loop-??(HVL-??) test facility. Phenomena of subcooling were observed using the techniques of planar laser induced fluorescent (PLIF), high speed photography, particle image velocimetry, etc. The flow and condition parameters were as follows: (1) CuCrZr alloy material, (2) triangle and rectangle fin structures, (3) inlet subcooling temperature of 296K, (4) Rhodamine solution flow velocity of 0.3~0.5m•s⁻¹. It was found that the heat transfer coefficient (HTC) of rectangle fin is 1.3??1.5 times higher than the triangle fin under the same tested conditions. Furthermore, the heat transfer efficiency is extraordinary dependent on the maintain time of vortex forming between the fins.     

聚变堆高热流部件超汽化换热实验研究

搭建了常压水超汽化实验回路(HVL-Ⅰ),采用平面激光诱导荧光(PLIF)、高速摄影、微距摄影、粒子成像测速(PIV)等先进测量技术,开展聚变堆面对等离子体部件(第一壁、偏滤器)在高热流过冷沸腾工况下强化换热特性实验研究。选择三角形和矩形翅片的铬锆铜超汽化样件,实验工况为常压室温(296K),若丹明B 水溶液流速 0.3～0.5m•s⁻¹ 连续可调,热流密度～5MW•m⁻²。实验结果表明同等工况下,矩形翅片比三角形翅片换热效果显著增强,性能提升约30%～50%。微距摄影显示翅根涡流形态保持时间越短,越有利于小汽泡充分扩散,从而使换热得到强化。     

Cs蒸气中的碰撞能量合并和6P3/2和6P1/2间的激发转移

通过激发转移和碰撞能量合并研究了Cs(62P)精细结构混合.单模半导体激光器激发基态Cs原子至6P3/2态,直接荧光是由6P3/2态发射的,敏化荧光是由精细结构碰撞转移和碰撞能量合并产生的.由相对荧光强度得到了转移截面σ(6P3/2→6P1/2)=(1.5±0.5)×10-15cm2,与其它实验结果进行了比较.     

Rb（5PJ）＋Rb（5PJ）→Rb（5JS）＋Rb（nl=5D，7S）碰撞能量合并

研究了Rb(5PJ)+Rb(5PJ)→Rb(nlJ')+Rb(5S)碰撞能量合并过程,利用单模半导体激光器分别共振激发Rb原子的5P1/2或5P3/2态,利用另一与泵浦激光束反向平行的单模激光束作为吸收线探测激发态原子密度及其空间分布,吸收线分别调至5P1/2→5D3/2和5P3/2→7S1/2跃迁.由激发态原子密度和谱线荧光比得到碰撞能量合并过程的截面,对5P3/2激发,碰撞转移得到5D5/2,5D3/2和7S1/2的截面分别是(1.32士0.59)×10-14,(1.18士0.53)×10-14和(3.21士1.44)×10-15cm2;对5P1/2激发,碰撞转移到5D5/2和5D3/2的截面分别是(6.57士2.96)×10-15和(5.90士2.66)×10-15cm2.与其他的实验结果进行了比较.     

Cs-He光学碰撞中的非绝热跃迁

激光激发Cs He碰撞复合物,测量了Cs(62P)精细结构布居数分支比,由此证实了发生在光学碰撞中的非绝热跃迁.激光频率从Cs(6P3/2)红翼30cm-1调至蓝翼30cm-1,在6P3/2的近翼,分支比与矢谐量有很大的关系.同时测量了Cs(6PJ)态的精细结构转移截面,截面值σ21=9.8×10-19cm2.     

环境中铬形态分析研究进展

对近10年来国内外在环境中铬形态方面的分析研究进展作了综述,内容包括样品预处理、分离富集方法和样品检测方法(引述文献61篇).     

激发态Cs(5D)原子间碰撞能量转移

用激光二步激发Cs原子至8S态,从谱线的波长及强度可以确定Cs原子的辐射及碰撞过程,5D态主要是由8S→7P→5D跃迁布居的.在1016-1017Cs密度范围内,测量了碰撞能量合并5D 5D→nL 6S(nL=9D,11S,7F)速率系数,因5D→6P(3.0-3.6μm)处于红外本实验不能探测,利用一个已经测量过的过程(即6P 5D→6S 7D)作相对测量,对于9D,11S和7F态,其平均速率系数分别为(8.4±4.2)×10-10,(7.3±3.6)×10-10和(9.7±4.8)×10-10cm3s-1.讨论了碰撞转移过程11S 6S 7F 6S对速率系数的影响.     

离子印迹壳聚糖/凹土分离富集-火焰原子吸收光谱测定中药材中痕量Cd(Ⅱ)的研究

建立了离子印迹壳聚糖/凹凸棒石(IICA)分离富集-火焰原子吸收光谱(FAAS)测定中药材中痕量Cd(Ⅱ)的新方法。在动态吸附条件下,系统研究了溶液pH值、流速、洗脱条件和干扰离子对痕量Cd(Ⅱ)分离富集的影响。研究表明,在pH为4.5,上样流速为0.60mL/min条件下,Cd(Ⅱ)能被IICA定量富集;吸附的Cd(Ⅱ)可用1.0mol/L HCl-0.1mol/L甲基异丁酮的乙醇溶液,在流速为0.96mL/min条件下完全洗脱。优化条件下,IICA对Cd(Ⅱ)的动态吸附容量为56.45mg/g。线性范围为0.00097～1.28mg/L,r=0.9994,检出限(3σ,n=11)为0.97μg/L,相对标准偏差为1.32%(n=6,c=0.08mg/L),回收率在96.5%～106.4%之间。该方法操作简便,灵敏度和精密度高,可应用于实际中药材样品中痕量镉的测定。     

Photoinitiated crosslinking of EPDM/inorganic filler blends and characterization of related properties

<正>Photoinitiated crosslinking of ethylene-propylene-diene terpolymer(EPDM) blends filled with calcium carbonate, talc and calcined kaolin(CK) in the presence of benzil dimethyl ketal as photoinitiator and trimethylolpropane triacrylate as crosslinker and their related properties have been studied by different analytical methods.The results from gel content and heat extension determination show that the efficiency of photocrosslinking of EPDM increases with increasing the content of diene and its molecular weight.The EPDM blends with 100 phr different inorganic fillers can be photocrosslinked to gel content of above 60%by 5 s UV-irradiation under optimum conditions.Under the same conditions of irradiation,the orders of photocrosslinking rate and final gel content are EPDM/CaCO_3EPDM/talcEPDM/CK.The data from thermogravimetric analysis,dynamic mechanical thermal analysis,electrical properties,mechanical tests and scanning electron microscopy show that UV irradiation crosslinking apparently enhances the thermal stability,mechanical properties and electrical properties of the photocrosslinked EPDM/inorganic filler samples.Although the attenuated total-reflection FTIR data show that inorganic fillers can promote the surface photo-oxidation of EPDM/inorganic filler samples with increasing the irradiation time,the above related properties of the photocrosslinked EPDM blends irradiated within 5 s are enough to satisfy many applications in the cable industry.     

单模光纤中三阶色散对超短光脉冲传输的影响

基于超短光脉冲在单模光纤中传输时高阶非线性效应的影响。应用非线性薛定谔方程(HONLS)理论,考虑光纤色散三阶效应,推导出无啁啾的高斯脉冲沿光纤传输时脉冲变化的表达式,并对理论结果进行了数值模拟与分析。结果表明,三阶色散会引起光脉冲形状发生畸变,会在其前沿或后沿附近形成非对称的振荡结构。